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Chiral Separation of Dextromethorphan/Levomethorphan and Dextrorphan/Levorphanol on Lux 3u AMP, 150x4.6mm

Sample Preparation Details

Application Detail (App ID: 25783)

Part No:00F-4751-E0
Dimensions:150 x 4.6 mm ID
Elution Type:Gradient
Elution A:5mM ammonium bicarbonate, adjusted to pH 11 with ammonium hydroxide
Elution B:Acetonitrile
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 55 45
2 4.5 55 45
3 4.6 20 80
4 8 20 80
5 8.1 55 45
6 10 55 45

Flow Rate:1 mL/min
Col. Temp: 40 °C
Detection: LC/MS/MS @ (0°C)
Note:Urine hydrolyzed with beta-glucuronidase and extracted with Strata-X-C

Analyte Details

Analyte Detail not available

1
Dextrorphan 1
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2
Dextrorphan 2
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3
Levorphanol 1
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4
Levorphanol 2
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5
Dextromethorphan 1
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6
Dextromethorphan 2
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7
Levomethorphan 1
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8
Levomethorphan 2
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